TA Instruments

AR1709-0001f

04/09/2012 16:51:02

Sample name	ASW 10 mm from base, 60 mm to top, disk 7 PMMA fouled AND DOUBLE CLEANED
Sample notes	 
Experiment notes	Plastic parallel plate with adaptor supplied by Southampton Uni., on ETC rod with grub screws.

Distances fromlower surface of PP plate. Southampton container.
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1709
Run number	1 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	04/09/2012 16:51:02

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	Yes
Initial temperature	22.4 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:01:00 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 3.000 rad/s
End controlled variable	velocity 300.0 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 300.0 rad/s
Duration	0:00:30 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	Yes
Ramp type	Continuous ramp
Start controlled variable	velocity 300.0 rad/s
End controlled variable	velocity 3.000 rad/s
Duration	0:01:00 hh:mm:ss
Ramp mode	linear 
Delay time	0:00:01 hh:mm:ss
Temperature	22.4 C
Wait for temperature	No
Match duration and start value to previous step	No
Motor mode	auto 

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	22.4 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	3.100 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.262 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	3
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	18.42 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Continuous ramp step 1

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

9.233	5.118	1.804	1.0160	22.4	454.7	1.6993	10000	0.1116	17.36	2.1242	212.42	3.383E-3	0.0	1.0	61.016	28.327	4.094
0.7436	12.44	0.05976	2.0200	22.4	467.1	13.3013	10000	0.1146	3.017	16.627	1662.7	3.384E-3	0.0	1.0	62.020	2.2814	9.954
1.536	19.37	0.07931	3.0160	22.4	463.8	26.9258	10000	0.1138	1.236	33.657	3365.7	3.383E-3	0.1	1.1	63.016	4.7139	15.50
2.071	23.05	0.08986	4.0240	22.4	467.9	41.1812	10000	0.1148	0.8806	51.477	5147.7	3.384E-3	0.1	1.1	64.024	6.3548	18.44
3.410	30.85	0.1105	5.0120	22.4	463.8	67.6340	10000	0.1138	0.4873	84.543	8454.3	3.383E-3	0.1	1.1	65.012	10.462	24.68
5.219	39.49	0.1322	6.0000	22.4	452.2	107.2720	10000	0.1110	0.2900	134.09	13409	3.383E-3	0.1	1.1	66.000	16.011	31.59
5.920	42.54	0.1392	7.0520	22.4	468.7	126.5600	10000	0.1150	0.2591	158.20	15820	3.384E-3	0.1	1.1	67.052	18.161	34.03
7.509	49.12	0.1529	8.0000	22.4	459.6	165.1870	10000	0.1128	0.1905	206.48	20648	3.384E-3	0.1	1.1	68.000	23.036	39.30
9.912	57.53	0.1723	9.0000	22.4	462.1	223.0860	10000	0.1134	0.1396	278.86	27886	3.384E-3	0.2	1.2	69.000	30.409	46.02
11.70	63.68	0.1838	10.012	22.4	463.8	274.6610	10000	0.1138	0.1143	343.33	34333	3.384E-3	0.2	1.2	70.012	35.903	50.95
13.54	69.65	0.1944	10.996	22.4	450.5	325.9620	10000	0.1106	0.09288	407.45	40745	3.383E-3	0.2	1.2	70.996	41.533	55.72
15.29	75.11	0.2036	12.024	22.4	450.5	377.1230	10000	0.1106	0.07985	471.40	47140	3.384E-3	0.2	1.2	72.024	46.910	60.09
17.33	80.51	0.2152	13.012	22.4	454.7	434.6430	10000	0.1116	0.07015	543.30	54330	3.384E-3	0.2	1.2	73.012	53.158	64.40
19.47	86.42	0.2252	14.020	22.4	447.2	498.4990	10000	0.1098	0.05988	623.12	62312	3.384E-3	0.2	1.2	74.020	59.720	69.14
22.48	94.60	0.2377	15.000	22.4	430.7	594.0700	10000	0.1057	0.04813	742.59	74259	3.384E-3	0.3	1.3	75.000	68.972	75.68
24.59	99.91	0.2461	16.000	22.4	429.0	664.7340	10000	0.1053	0.04298	830.92	83092	3.384E-3	0.3	1.3	76.000	75.436	79.93
26.82	105.7	0.2538	17.020	22.4	447.2	740.5420	10000	0.1098	0.04006	925.68	92568	3.384E-3	0.3	1.3	77.020	82.276	84.52
30.28	113.7	0.2663	18.012	22.4	429.0	854.8870	10000	0.1053	0.03317	1068.6	1.0686E5	3.383E-3	0.3	1.3	78.012	92.897	90.98
32.38	118.8	0.2726	19.008	22.4	419.1	932.0070	10000	0.1029	0.02970	1165.0	1.1650E5	3.384E-3	0.3	1.3	79.008	99.346	95.03
34.63	124.2	0.2787	20.008	22.4	419.1	1019.9800	10000	0.1029	0.02715	1275.0	1.2750E5	3.383E-3	0.3	1.3	80.008	106.24	99.39
38.60	132.3	0.2918	21.016	22.4	419.9	1153.2000	10000	0.1031	0.02400	1441.5	1.4415E5	3.384E-3	0.4	1.4	81.016	118.42	105.8
41.00	137.4	0.2985	22.000	22.4	406.7	1242.0300	10000	0.09982	0.02155	1552.5	1.5525E5	3.384E-3	0.4	1.4	82.000	125.80	109.9
43.31	142.8	0.3033	22.996	22.4	412.5	1343.5500	10000	0.1012	0.02023	1679.4	1.6794E5	3.384E-3	0.4	1.4	82.996	132.88	114.2
47.39	150.8	0.3142	24.012	22.4	420.8	1495.8500	10000	0.1033	0.01850	1869.8	1.8698E5	3.384E-3	0.4	1.4	84.012	145.38	120.6
50.18	155.9	0.3218	24.992	22.4	396.8	1596.9000	10000	0.09739	0.01632	1996.1	1.9961E5	3.384E-3	0.4	1.4	84.992	153.95	124.7
53.28	161.3	0.3303	26.012	22.4	394.3	1710.8900	10000	0.09678	0.01515	2138.6	2.1386E5	3.384E-3	0.4	1.4	86.012	163.47	129.1
57.28	169.3	0.3383	27.000	22.4	395.1	1881.8600	10000	0.09698	0.01378	2352.3	2.3523E5	3.384E-3	0.5	1.5	87.000	175.73	135.5
59.91	174.4	0.3434	28.012	22.4	400.1	1995.7400	10000	0.09820	0.01315	2494.7	2.4947E5	3.383E-3	0.5	1.5	88.012	183.79	139.6
63.07	179.6	0.3512	29.012	22.4	390.2	2116.0000	10000	0.09576	0.01210	2645.0	2.6450E5	3.383E-3	0.5	1.5	89.012	193.49	143.6
67.86	187.6	0.3618	30.024	22.4	385.2	2305.7400	10000	0.09455	0.01095	2882.2	2.8822E5	3.384E-3	0.5	1.5	90.024	208.21	150.0
70.91	192.7	0.3680	31.000	22.4	385.2	2432.2800	10000	0.09455	0.01037	3040.4	3.0404E5	3.383E-3	0.5	1.5	91.000	217.55	154.2
73.78	197.8	0.3730	32.008	22.4	381.1	2636.3000	10000	0.09353	9.737E-3	3295.4	3.2954E5	3.384E-3	0.5	1.5	92.008	226.37	158.3
78.39	205.8	0.3808	33.000	22.4	352.2	2773.7600	10000	0.08643	8.313E-3	3467.2	3.4672E5	3.383E-3	0.6	1.6	93.000	240.48	164.7
82.21	211.0	0.3897	33.996	22.4	371.2	2913.5100	10000	0.09110	8.338E-3	3641.9	3.6419E5	3.383E-3	0.6	1.6	93.996	252.22	168.8
85.76	218.6	0.3923	35.020	22.4	362.9	3128.7700	10000	0.08907	7.594E-3	3911.0	3.9110E5	3.384E-3	0.6	1.6	95.020	263.11	174.9
89.86	223.9	0.4013	36.020	22.4	356.3	3279.1101	10000	0.08745	7.107E-3	4098.9	4.0989E5	3.384E-3	0.6	1.6	96.020	275.69	179.1
93.82	231.6	0.4051	37.028	22.4	345.5	3507.7500	10000	0.08481	6.441E-3	4384.7	4.3847E5	3.383E-3	0.6	1.6	97.028	287.85	185.3
98.38	236.6	0.4158	38.036	22.4	338.1	3658.0500	10000	0.08298	6.038E-3	4572.6	4.5726E5	3.384E-3	0.6	1.6	98.036	301.84	189.3
102.3	241.8	0.4230	39.000	22.4	362.1	3822.2200	10000	0.08887	6.191E-3	4777.8	4.7778E5	3.384E-3	0.7	1.7	99.000	313.82	193.5
106.7	249.6	0.4273	40.016	22.4	345.5	4068.5701	10000	0.08481	5.547E-3	5085.7	5.0857E5	3.384E-3	0.7	1.7	100.016	327.22	199.7
109.3	254.6	0.4291	41.000	22.4	329.8	4232.6499	10000	0.08095	5.088E-3	5290.8	5.2908E5	3.384E-3	0.7	1.7	101.000	335.22	203.7
115.5	262.5	0.4401	42.020	22.4	336.4	4499.4199	10000	0.08258	4.884E-3	5624.3	5.6243E5	3.384E-3	0.7	1.7	102.020	354.38	210.0
120.3	267.6	0.4496	43.012	22.4	320.7	4674.4800	10000	0.07872	4.479E-3	5843.1	5.8431E5	3.383E-3	0.7	1.7	103.012	369.11	214.1
124.4	272.7	0.4562	44.012	22.4	324.9	4851.2998	10000	0.07974	4.370E-3	6064.1	6.0641E5	3.384E-3	0.7	1.7	104.012	381.64	218.1
128.5	280.3	0.4583	45.012	22.4	323.2	5129.2002	10000	0.07933	4.112E-3	6411.5	6.4115E5	3.384E-3	0.8	1.8	105.012	394.18	224.3
132.7	285.5	0.4647	46.008	22.4	319.1	5318.3701	10000	0.07832	3.914E-3	6648.0	6.6480E5	3.383E-3	0.8	1.8	106.008	407.06	228.4
137.7	293.1	0.4696	47.020	22.4	323.2	5602.3398	10000	0.07933	3.762E-3	7002.9	7.0029E5	3.384E-3	0.8	1.8	107.020	422.30	234.5
142.9	298.1	0.4794	48.012	22.4	300.9	5797.7998	10000	0.07385	3.385E-3	7247.3	7.2473E5	3.383E-3	0.8	1.8	108.012	438.55	238.5
146.6	303.3	0.4833	49.016	22.4	291.0	6101.9502	10000	0.07142	3.162E-3	7627.4	7.6274E5	3.383E-3	0.8	1.8	109.016	449.74	242.7
152.1	311.0	0.4890	50.016	22.4	281.9	6304.3799	10000	0.06919	2.915E-3	7880.5	7.8805E5	3.383E-3	0.8	1.8	110.016	466.52	248.8
156.1	316.0	0.4940	51.000	22.4	291.0	6511.5898	10000	0.07142	2.914E-3	8139.5	8.1395E5	3.383E-3	0.9	1.9	111.000	478.96	252.8
162.8	323.8	0.5028	52.020	22.4	273.6	6833.5298	10000	0.06716	2.610E-3	8541.9	8.5419E5	3.384E-3	0.9	1.9	112.020	499.50	259.0
166.5	328.9	0.5064	53.012	22.4	275.3	7047.4800	10000	0.06756	2.545E-3	8809.4	8.8094E5	3.384E-3	0.9	1.9	113.012	510.95	263.1
173.8	336.4	0.5166	54.012	22.4	298.4	7376.5498	10000	0.07324	2.637E-3	9220.7	9.2207E5	3.383E-3	0.9	1.9	114.012	533.21	269.1
177.1	341.6	0.5184	54.996	22.4	261.2	7601.4902	10000	0.06411	2.239E-3	9501.9	9.5019E5	3.383E-3	0.9	1.9	114.996	543.33	273.3
181.0	346.7	0.5220	55.996	22.4	276.1	7832.6099	10000	0.06777	2.297E-3	9790.8	9.7908E5	3.384E-3	0.9	1.9	115.996	555.25	277.4
188.0	354.2	0.5306	57.024	22.4	265.4	8168.8398	10000	0.06513	2.115E-3	10211	1.0211E6	3.384E-3	1.0	2.0	117.024	576.64	283.4
191.9	359.4	0.5340	57.996	22.4	260.4	8408.5195	10000	0.06391	2.016E-3	10511	1.0511E6	3.384E-3	1.0	2.0	117.996	588.67	287.5
201.5	367.0	0.5489	59.012	22.4	233.1	8767.7695	10000	0.05722	1.731E-3	10960	1.0960E6	3.384E-3	1.0	2.0	119.012	618.05	293.6
203.0	372.0	0.5456	59.996	22.4	264.5	9007.1201	10000	0.06493	1.912E-3	11259	1.1259E6	3.384E-3	1.0	2.0	119.996	622.64	297.6

Peak hold step

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

208.2	375.0	0.5551	0.99200	22.4	255.4	278.3980	10000	0.06269	1.817E-3	348.00	34800	3.384E-3	0.0	2.0	121.992	638.61	300.0
207.4	375.0	0.5530	2.0040	22.4	251.3	529.8600	10000	0.06168	1.787E-3	662.33	66233	3.384E-3	0.0	2.1	123.004	636.26	300.0
208.7	375.0	0.5564	2.9960	22.4	238.9	906.6410	10000	0.05864	1.699E-3	1133.3	1.1333E5	3.384E-3	0.0	2.1	123.996	640.15	300.0
207.8	375.0	0.5541	4.0000	22.4	219.9	1158.1400	10000	0.05397	1.564E-3	1447.7	1.4477E5	3.384E-3	0.1	2.1	125.000	637.45	300.0
207.6	375.0	0.5537	4.9920	22.4	246.3	1409.5900	10000	0.06046	1.752E-3	1762.0	1.7620E5	3.384E-3	0.1	2.1	125.992	636.97	300.0
206.0	375.0	0.5493	5.9920	22.4	252.1	1786.4399	10000	0.06188	1.793E-3	2233.1	2.2331E5	3.384E-3	0.1	2.1	126.992	632.02	300.0
210.6	375.0	0.5617	6.9920	22.4	191.8	2037.7300	10000	0.04707	1.364E-3	2547.2	2.5472E5	3.383E-3	0.1	2.1	127.992	646.20	300.0
207.6	375.0	0.5536	7.9920	22.4	205.0	2292.7600	10000	0.05032	1.458E-3	2866.0	2.8660E5	3.384E-3	0.1	2.1	128.992	636.95	300.0
204.4	375.0	0.5450	9.0000	22.4	215.8	2667.4199	10000	0.05295	1.534E-3	3334.3	3.3343E5	3.383E-3	0.2	2.2	130.000	627.06	300.0
205.1	375.0	0.5468	9.9920	22.4	225.7	2920.9700	10000	0.05539	1.605E-3	3651.2	3.6512E5	3.384E-3	0.2	2.2	130.992	629.10	300.0
208.4	375.0	0.5556	10.988	22.4	216.6	3294.3301	10000	0.05316	1.540E-3	4117.9	4.1179E5	3.383E-3	0.2	2.2	131.988	639.24	300.0
206.0	375.0	0.5494	12.000	22.4	260.4	3546.5901	10000	0.06391	1.852E-3	4433.2	4.4332E5	3.383E-3	0.2	2.2	133.000	632.10	300.0
206.1	375.0	0.5495	12.992	22.4	233.9	3797.0500	10000	0.05742	1.664E-3	4746.3	4.7463E5	3.384E-3	0.2	2.2	133.992	632.23	300.0
209.0	375.0	0.5574	14.000	22.4	205.0	4175.8799	10000	0.05032	1.458E-3	5219.9	5.2199E5	3.384E-3	0.2	2.3	135.000	641.29	300.0
205.6	375.0	0.5484	14.992	22.4	243.0	4425.2402	10000	0.05965	1.728E-3	5531.6	5.5316E5	3.384E-3	0.2	2.3	135.992	630.90	300.0
210.5	375.0	0.5613	16.004	22.4	230.6	4804.0298	10000	0.05661	1.640E-3	6005.0	6.0050E5	3.384E-3	0.3	2.3	137.004	645.78	300.0
207.0	375.0	0.5519	16.992	22.4	252.1	5053.5898	10000	0.06188	1.793E-3	6317.0	6.3170E5	3.384E-3	0.3	2.3	137.992	634.96	300.0
210.1	375.0	0.5604	17.992	22.4	236.4	5306.2402	10000	0.05803	1.681E-3	6632.8	6.6328E5	3.384E-3	0.3	2.3	138.992	644.68	300.0
204.7	375.0	0.5459	19.000	22.4	271.1	5682.0298	10000	0.06655	1.928E-3	7102.5	7.1025E5	3.384E-3	0.3	2.3	140.000	628.07	300.0
206.6	375.0	0.5511	19.996	22.4	238.9	5933.3198	10000	0.05864	1.699E-3	7416.7	7.4167E5	3.384E-3	0.3	2.3	140.996	633.99	300.0
209.3	375.0	0.5582	20.992	22.4	221.5	6310.3799	10000	0.05437	1.576E-3	7888.0	7.8880E5	3.384E-3	0.3	2.4	141.992	642.23	300.0
208.8	375.0	0.5569	21.992	22.4	222.4	6561.5801	10000	0.05458	1.581E-3	8202.0	8.2020E5	3.384E-3	0.4	2.4	142.992	640.74	300.0
209.2	375.0	0.5580	22.992	22.4	210.8	6813.0000	10000	0.05174	1.499E-3	8516.3	8.5163E5	3.384E-3	0.4	2.4	143.992	641.95	300.0
208.8	375.0	0.5567	24.000	22.4	208.3	7190.0098	10000	0.05113	1.481E-3	8987.5	8.9875E5	3.384E-3	0.4	2.4	145.000	640.44	300.0
210.1	375.0	0.5602	24.992	22.4	205.0	7443.4702	10000	0.05032	1.458E-3	9304.3	9.3043E5	3.383E-3	0.4	2.4	145.992	644.46	300.0
211.8	375.0	0.5647	25.992	22.4	217.4	7820.5400	10000	0.05336	1.546E-3	9775.7	9.7757E5	3.384E-3	0.4	2.4	146.992	649.73	300.0
208.3	375.0	0.5554	26.992	22.4	208.3	8069.5098	10000	0.05113	1.481E-3	10087	1.0087E6	3.384E-3	0.4	2.5	147.992	639.04	300.0
206.4	375.0	0.5504	27.992	22.4	259.6	8321.1504	10000	0.06371	1.846E-3	10401	1.0401E6	3.384E-3	0.5	2.5	148.992	633.18	300.0
208.2	375.0	0.5552	28.996	22.4	237.2	8697.9805	10000	0.05823	1.687E-3	10872	1.0872E6	3.384E-3	0.5	2.5	149.996	638.72	300.0
209.7	375.0	0.5591	29.992	22.4	228.2	8949.1396	10000	0.05600	1.623E-3	11186	1.1186E6	3.384E-3	0.5	2.5	150.992	643.26	300.0

Continuous ramp step 2

shear stress	shear rate	viscosity	time	temperature	normal stress	displacement	gap	normal force	normal stress coefficient	strain	% strain	1/temperature	time	time global	time global	torque	velocity
Pa	1/s	Pa.s	s	C	Pa	rad	micro m	N	Pa.s^2			1/K	min	min	s	micro N.m	rad/s

202.6	370.1	0.5475	1.0080	22.4	251.3	313.5670	10000	0.06168	1.834E-3	391.96	39196	3.384E-3	0.0	2.5	152.008	621.69	296.1
199.0	365.1	0.5450	2.0120	22.4	233.1	550.6020	10000	0.05722	1.749E-3	688.25	68825	3.384E-3	0.0	2.6	153.012	610.53	292.1
191.7	360.1	0.5324	3.0080	22.4	253.8	788.4720	10000	0.06229	1.957E-3	985.59	98559	3.383E-3	0.1	2.6	154.008	588.10	288.1
184.2	352.3	0.5229	4.0120	22.4	284.4	1145.4100	10000	0.06979	2.291E-3	1431.8	1.4318E5	3.384E-3	0.1	2.6	155.012	565.21	281.9
181.5	347.3	0.5227	5.0080	22.4	249.6	1370.7800	10000	0.06127	2.070E-3	1713.5	1.7135E5	3.383E-3	0.1	2.6	156.008	556.88	277.8
177.5	339.6	0.5225	6.0080	22.4	268.7	1708.9800	10000	0.06594	2.329E-3	2136.2	2.1362E5	3.383E-3	0.1	2.6	157.008	544.49	271.7
170.8	334.5	0.5105	7.0080	22.4	296.8	1934.1801	10000	0.07284	2.653E-3	2417.7	2.4177E5	3.383E-3	0.1	2.6	158.008	523.89	267.6
162.0	326.9	0.4954	8.0120	22.4	310.8	2253.6399	10000	0.07629	2.908E-3	2817.1	2.8171E5	3.384E-3	0.1	2.7	159.012	496.93	261.5
160.0	321.9	0.4971	9.0080	22.4	291.0	2466.4600	10000	0.07142	2.809E-3	3083.1	3.0831E5	3.384E-3	0.2	2.7	160.008	490.87	257.5
156.0	316.7	0.4925	10.008	22.4	284.4	2679.1699	10000	0.06979	2.835E-3	3349.0	3.3490E5	3.384E-3	0.2	2.7	161.008	478.54	253.4
150.9	309.0	0.4884	11.008	22.4	273.6	2985.9600	10000	0.06716	2.865E-3	3732.5	3.7325E5	3.384E-3	0.2	2.7	162.008	463.01	247.2
148.0	304.0	0.4868	12.008	22.4	303.4	3186.2400	10000	0.07446	3.283E-3	3982.8	3.9828E5	3.384E-3	0.2	2.7	163.008	454.00	243.2
138.6	296.2	0.4680	13.008	22.4	313.3	3487.7700	10000	0.07690	3.570E-3	4359.7	4.3597E5	3.383E-3	0.2	2.7	164.008	425.34	237.0
137.2	291.0	0.4715	14.008	22.4	293.5	3682.1399	10000	0.07203	3.465E-3	4602.7	4.6027E5	3.383E-3	0.2	2.8	165.008	421.03	232.8
132.6	283.5	0.4676	15.016	22.4	321.6	3962.8701	10000	0.07892	4.002E-3	4953.6	4.9536E5	3.383E-3	0.3	2.8	166.016	406.69	226.8
128.8	278.3	0.4628	16.008	22.4	305.9	4149.7598	10000	0.07507	3.949E-3	5187.2	5.1872E5	3.383E-3	0.3	2.8	167.008	395.15	222.6
123.5	273.1	0.4521	17.008	22.4	335.6	4331.3101	10000	0.08237	4.499E-3	5414.1	5.4141E5	3.383E-3	0.3	2.8	168.008	378.83	218.5
117.6	265.6	0.4429	18.012	22.4	324.9	4593.9302	10000	0.07974	4.606E-3	5742.4	5.7424E5	3.383E-3	0.3	2.8	169.012	360.89	212.5
112.7	260.4	0.4328	19.008	22.4	352.2	4768.9600	10000	0.08643	5.192E-3	5961.2	5.9612E5	3.383E-3	0.3	2.8	170.008	345.83	208.3
108.2	252.6	0.4284	20.016	22.4	336.4	5025.5601	10000	0.08258	5.273E-3	6282.0	6.2820E5	3.384E-3	0.3	2.9	171.016	332.02	202.1
105.1	247.6	0.4244	21.024	22.4	338.9	5188.0898	10000	0.08319	5.530E-3	6485.1	6.4851E5	3.383E-3	0.4	2.9	172.024	322.32	198.1
100.4	242.4	0.4143	22.008	22.4	349.7	5351.3398	10000	0.08582	5.950E-3	6689.2	6.6892E5	3.383E-3	0.4	2.9	173.008	308.14	193.9
96.07	234.5	0.4097	23.008	22.4	350.5	5594.2598	10000	0.08603	6.372E-3	6992.8	6.9928E5	3.384E-3	0.4	2.9	174.008	294.75	187.6
91.55	226.9	0.4035	24.192	22.4	348.0	5819.4199	10000	0.08542	6.761E-3	7274.3	7.2743E5	3.384E-3	0.4	2.9	175.192	280.87	181.5
87.62	221.7	0.3952	25.100	22.4	372.0	5969.3101	10000	0.09130	7.568E-3	7461.6	7.4616E5	3.384E-3	0.4	2.9	176.100	268.80	177.4
84.41	216.4	0.3901	26.008	22.4	358.8	6119.2002	10000	0.08805	7.661E-3	7649.0	7.6490E5	3.384E-3	0.4	3.0	177.008	258.97	173.1
81.95	211.3	0.3878	27.008	22.4	391.0	6256.7798	10000	0.09597	8.756E-3	7821.0	7.8210E5	3.384E-3	0.5	3.0	178.008	251.42	169.1
76.45	203.6	0.3754	28.004	22.4	384.4	6462.8198	10000	0.09434	9.270E-3	8078.5	8.0785E5	3.384E-3	0.5	3.0	179.004	234.54	162.9
72.17	198.3	0.3638	29.008	22.4	371.2	6600.6299	10000	0.09110	9.434E-3	8250.8	8.2508E5	3.384E-3	0.5	3.0	180.008	221.41	158.7
69.55	193.0	0.3603	30.008	22.4	379.4	6794.4800	10000	0.09313	0.01018	8493.1	8.4931E5	3.384E-3	0.5	3.0	181.008	213.39	154.4
66.65	185.4	0.3595	31.008	22.4	387.7	6918.5200	10000	0.09516	0.01128	8648.2	8.6482E5	3.384E-3	0.5	3.0	182.008	204.48	148.3
62.23	180.1	0.3455	32.008	22.4	404.2	7043.2900	10000	0.09921	0.01246	8804.1	8.8041E5	3.384E-3	0.5	3.1	183.008	190.90	144.1
58.46	172.3	0.3393	33.020	22.4	402.6	7218.0801	10000	0.09881	0.01356	9022.6	9.0226E5	3.384E-3	0.6	3.1	184.020	179.35	137.8
55.73	167.2	0.3333	34.008	22.4	409.2	7330.3799	10000	0.1004	0.01464	9163.0	9.1630E5	3.384E-3	0.6	3.1	185.008	170.96	133.7
52.35	161.9	0.3234	34.992	22.4	396.0	7443.3501	10000	0.09718	0.01511	9304.2	9.3042E5	3.384E-3	0.6	3.1	185.992	160.61	129.5
48.07	153.8	0.3125	35.992	22.4	409.2	7604.6299	10000	0.1004	0.01730	9505.8	9.5058E5	3.384E-3	0.6	3.1	186.992	147.47	123.0
45.43	148.7	0.3055	36.992	22.4	410.0	7704.3599	10000	0.1006	0.01854	9630.5	9.6305E5	3.384E-3	0.6	3.1	187.992	139.37	119.0
43.55	143.4	0.3037	38.008	22.4	428.2	7803.9902	10000	0.1051	0.02082	9755.0	9.7550E5	3.384E-3	0.6	3.2	189.008	133.61	114.7
39.53	135.3	0.2921	39.012	22.4	424.1	7947.2100	10000	0.1041	0.02317	9934.0	9.9340E5	3.384E-3	0.7	3.2	190.012	121.26	108.2
37.46	130.2	0.2876	40.012	22.4	428.2	8034.3599	10000	0.1051	0.02525	10043	1.0043E6	3.384E-3	0.7	3.2	191.012	114.91	104.2
34.93	124.9	0.2796	41.008	22.4	418.3	8121.4199	10000	0.1027	0.02680	10152	1.0152E6	3.384E-3	0.7	3.2	192.008	107.17	99.95
32.26	116.6	0.2767	41.992	22.4	436.5	8252.4697	10000	0.1071	0.03212	10316	1.0316E6	3.383E-3	0.7	3.2	192.992	98.962	93.25
29.40	111.3	0.2642	43.008	22.4	425.7	8327.0703	10000	0.1045	0.03437	10409	1.0409E6	3.383E-3	0.7	3.2	194.008	90.200	89.03
27.10	106.0	0.2557	44.008	22.4	427.4	8401.2002	10000	0.1049	0.03805	10502	1.0502E6	3.384E-3	0.7	3.3	195.008	83.142	84.78
24.29	100.4	0.2420	45.008	22.4	426.6	8475.9004	10000	0.1047	0.04232	10595	1.0595E6	3.383E-3	0.8	3.3	196.008	74.528	80.32
21.55	92.18	0.2337	46.008	22.4	437.3	8574.7900	10000	0.1073	0.05147	10718	1.0718E6	3.383E-3	0.8	3.3	197.008	66.102	73.74
19.36	86.82	0.2230	47.008	22.4	433.2	8636.9102	10000	0.1063	0.05747	10796	1.0796E6	3.383E-3	0.8	3.3	198.008	59.394	69.45
17.25	81.12	0.2126	48.008	22.4	440.6	8698.5000	10000	0.1081	0.06696	10873	1.0873E6	3.383E-3	0.8	3.3	199.008	52.912	64.89
14.88	75.32	0.1975	49.008	22.4	436.5	8754.0303	10000	0.1071	0.07694	10943	1.0943E6	3.383E-3	0.8	3.3	200.008	45.647	60.25
12.51	67.28	0.1859	50.008	22.4	437.3	8828.0898	10000	0.1073	0.09661	11035	1.1035E6	3.383E-3	0.8	3.4	201.008	38.381	53.82
10.65	61.36	0.1736	51.008	22.4	451.4	8877.1797	10000	0.1108	0.1199	11096	1.1096E6	3.383E-3	0.9	3.4	202.008	32.677	49.09
8.793	55.26	0.1591	52.016	22.4	451.4	8920.0801	10000	0.1108	0.1478	11150	1.1150E6	3.383E-3	0.9	3.4	203.016	26.975	44.21
7.487	49.84	0.1502	53.008	22.4	454.7	8956.8096	10000	0.1116	0.1830	11196	1.1196E6	3.383E-3	0.9	3.4	204.008	22.969	39.87
5.957	43.79	0.1360	54.008	22.4	463.8	8993.2803	10000	0.1138	0.2418	11242	1.1242E6	3.383E-3	0.9	3.4	205.008	18.275	35.03
4.454	37.46	0.1189	55.008	22.4	458.0	9023.5498	10000	0.1124	0.3263	11279	1.1279E6	3.383E-3	0.9	3.4	206.008	13.665	29.97
3.437	32.06	0.1072	56.008	22.4	450.5	9047.7002	10000	0.1106	0.4383	11310	1.1310E6	3.383E-3	0.9	3.5	207.008	10.546	25.65
2.416	25.64	0.09422	57.008	22.4	458.8	9071.4102	10000	0.1126	0.6977	11339	1.1339E6	3.383E-3	1.0	3.5	208.008	7.4124	20.51
1.944	21.82	0.08910	58.012	22.4	452.2	9082.9697	10000	0.1110	0.9496	11354	1.1354E6	3.383E-3	1.0	3.5	209.012	5.9654	17.46
0.8422	13.19	0.06386	59.024	22.4	461.3	9099.5498	10000	0.1132	2.652	11374	1.1374E6	3.384E-3	1.0	3.5	210.024	2.5837	10.55
0.1890	5.595	0.03377	60.016	22.4	458.8	9107.1396	10000	0.1126	14.65	11384	1.1384E6	3.384E-3	1.0	3.5	211.016	0.57971	4.476

